油炸和膨化食品中氯丙醇酯及缩水甘油酯污染调查研究
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唐山市疾病预防控制中心

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Contamination analysis of chloropropanol esters and glycidyl esters in fried food and puffed food
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Tangshan Center for Disease Control and Prevention

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    摘要:

    目的 调查油炸及膨化食品中3-氯丙醇酯(3-MCPDE)、2-氯丙醇酯(2-MCPDE)和缩水甘油酯(GE)的污染状况,为油炸及膨化食品中MCPDE和GE风险评估提供数据参考。方法 建立油炸和膨化食品中氯丙醇酯及缩水甘油酯同位素稀释气相色谱-串联质谱法,对55份油炸食品和66份膨化食品进行定量检测及污染水平分析。结果 油炸和膨化食品中3-MCPDE、2-MCPDE和GE检出率均为100%,油炸食品中3-MCPDE、2-MCPDE和GE含量范围分别为0.0525~1.59、0.0232~0.798和0.0257~3.06 mg/kg。膨化食品中3-MCPDE、2-MCPDE和GE含量范围为0.0892~2.31、0.0477~0.867和0.0755~2.58mg/kg。结论 MCPDE和GE含量水平均呈现膨化食品高于油炸食品的趋势,对膨化食品中MCPDE和GE的污染需要优先关注。

    Abstract:

    Objective To analyze the contamination levels of 3-MCPDE, 2-MCPDE and GE in fried food and puffed food, and we could provide a scientific basis for conducting risk assessment to the exposure levels of MCPDE and GE. Methods We detected chloropropanol esters and glycidyl esters by isotope dilution gas chromatography - tandem mass spectrometry and conducted an analysis of 3-MCPDE, 2-MCPDE and GE contamination levels in 55 fried food samples and 66 puffed food samples . Results The detection rates of 3-MCPDE, 2-MCPDE and GE in fried food and puffed food were all 100%, and the concent range of 3-MCPDE, 2-MCPDE and GE in fried food were from 0.0525 to 1.59, from 0.0232 to 0.798 and from 0.0257 to 3.06 mg/kg. The concent range of 3-MCPDE, 2-MCPDE and GE in puffed food were 0.0892 - 2.31, 0.0477 - 0.867 and 0.0755-2.58 mg/kg. Conclusion The results indicated that the contamination levels of 3-MCPDE, 2-MCPDE and GE in puffed food were higher than fried food, and we should put more attention on MCPDE and GE contamination in puffed food.

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  • 收稿日期:2025-02-10
  • 最后修改日期:2025-03-16
  • 录用日期:2025-03-17
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