2023年河南省小麦及其制品中交链孢毒素抽查复检结果分析与评价方法建立
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作者:
作者单位:

河南省疾病预防控制中心,河南 郑州 450016

作者简介:

张洁 女 副主任技师 研究方向为食品安全风险监测 E-mail:yuli2009@163.com

通讯作者:

翟志雷 男 副主任技师 研究方向为食品安全风险监测 E-mail:H52462673@163.com

中图分类号:

R155

基金项目:

河南省医学科技攻关计划联合共建项目(LHGJ20240613;LHGJ20240621)


Analysis and invaluation method establishment of aflatoxin re-inspection results in wheat and its products in He’nan Province in 2023
Author:
Affiliation:

He’nan Provincial Center for Disease Control and Prevention, He’nan Zhengzhou 450016, China

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    摘要:

    目的 分析2023年河南省小麦及其制品中4种交链孢毒素监测的复检结果,建立简单的质量评价方法。方法 国家常规及省专项应急项目共抽检省内15个地市的小麦及其制品51份。利用液相色谱-串联质谱内标法同时对样品中交链孢菌酮酸(TeA)、T-2毒素(TEN)、交链孢酚(AOH)、交链孢酚单甲醚(AME)进行复测,对两次检测结果的相对偏差(RD)进行归类统计分析,评价不同检测机构及检测项目的检测情况。结果 省疾控实验室在控制数据变异性方面表现较好,60.4%RD数据点在30%以内,专项实验室次之,9个地市实验室最低;4个检测项目中TeA和TEN灵敏度高,响应好,比较稳定,64.7%的RD数据点在30%以内,AOH和AME相对较差;结果数值的数量级越高,检测结果的一致性和可靠性越佳。结论 RD分层表示检测数据良好度可以反映检测过程的一致性和准确性,以及检测项目的质量控制水平。通过分析不同检测项目的RD,可以有效地识别检测质量,大部分样品的检测结果具有较高的一致性,表明检测机构整体表现良好,某些检测项目或地区存在较高的RD,需要更多的关注或改进,进一步调查原因,并采取相应的措施来减少变异性,为后续的质量控制提供依据。

    Abstract:

    Objective To analyze the re-inspection results of 4 types of aflatoxins in wheat and its products inspected in He’nan Province in 2023,a simple evaluation method was attempted to establish.Methods A total of 51 samples of wheat and its products were sampled from 15 cities within the province for national routine and provincial emergency monitoring projects. Simultaneous retesting of aflatoxin tricothecene A (TeA), T-2 toxin(TEN), ochratoxinA (AOH) and ochratoxin A methyl ester (AME) in the sample was conducted using liquid chromatography-tandem mass spectrometry with internal standardmethod. The relativedeviation(RD) between the two detection results was classified and statistically analyzed to evaluate the detection performance of different detection institutions and projects.Results The provincial disease control laboratory showed better performance in controlling data variability, with 60.4% of RD data points within 30%, followed by the special project laboratory and the nine prefecture-level city laboratories showed the lowest performance. Among the four detection projects, TeA and TEN showed high sensitivity and good response, with 64.7% of RD data points within 30%, while AOH and AME showed relatively poor performance. The higher the order of magnitude of the result value, the better the consistency and reliability of the detection results.Conclusion The stratification of RD indicates the quality of detection data, reflecting the consistency and accuracy of the detection process and the level of quality control of the detection projects. By analyzing the RD of different detection projects, the detection quality can be effectively identified. Most of the detection results of the samples have high consistency, indicating that the detection institutions have performed well overall. However, some detection projects or areas have higher relative deviations, requiring more attention and improvement. Further investigation of the causes and adoption of corresponding measures to reduce variability is needed to provide a basis for subsequent quality control.

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张洁,翟志雷,张秀丽,马青青,王谢,苏永恒.2023年河南省小麦及其制品中交链孢毒素抽查复检结果分析与评价方法建立[J].中国食品卫生杂志,2025,37(1):55-59.

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  • 收稿日期:2024-07-19
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  • 在线发布日期: 2025-05-16
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