低场核磁共振技术快速鉴别注水注胶肉的化学计量学研究
作者:
作者单位:

南京海关动植食中心,江苏 南京 210019

作者简介:

徐瑞平 男 副主任技师 研究方向为食品卫生及其风险评估 E-mail: njciq@foxmail.com

通讯作者:

丁涛 男 研究员 研究方向为食品分析与食品掺假鉴别 E-mail: nanoding@sina.com

中图分类号:

R155

基金项目:

海关总署科研项目(2021HK193);国家重点研发计划(2018YFC1603501)


Rapid identification of water-injected pork and gum-injected pork by the combination of low field nuclear magnetic resonance and chemometrics analysis
Author:
Affiliation:

Testing Center of Animal, Plant and Food, Nanjing Customs, Jiangsu Nanjing 210019, China

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    摘要:

    目的 利用化学计量学方法结合低场核磁共振对注水或注胶猪肉的快速鉴别进行研究。方法 首先利用低场核磁共振测定获得的17个变量进行提取主成分,并对获得的4个主成分进行判别研究模型。利用低场核磁共振技术的17个原始变量作为输入,原料肉与注水注胶肉的种类作为输出,采用不同建模参数,通过多次计算,建立了一个结构为17-6-3的三层MLP神经网络识别模型。结果 判别研究模型中对照组、注水组和注胶组交叉验证判别正确率分别为60/60、91/95、359/384,总的正确判别率达到94.6%;神经网络识别模型对检验集179个样本总的正确识别率达到97.8%。结论 利用低场核磁共振技术结合判别研究模型和神经网络识别模型可以有效分辨注水注胶肉,该方法具有简单、快速的优点,可以用于注水注胶肉的快速检测。

    Abstract:

    Objective To apply rapid identification of water-injected and gum-injected pork by chemometrics analysis combined with low field nuclear magnetic resonance.Methods 17 variables obtained by low field nuclear magnetic resonance were used to extract principal components by principal component analysis, and 4 principal components were identified by discriminate analysis. A three-layer MLP neural network model with a structure of 17-6-3 was established through constrained optimization modeling using 17 original variables as input, and the types of water-injected pork and gum-injected pork as output.Results In the discriminate analysis model, the discriminant accuracy of cross-validation in the control group, water-injected group and gum-injected group was 60/60, 91/95 and 359/384, and the total correct discriminant rate was 94.6%. In the neural network model, the total correct discriminant rate of 179 samples in the testing set was 97.8%.Conclusion Low-field nuclear magnetic resonance combined with discriminate analysis model and neural network model can effectively distinguish water-injected and gum-injected pork. The method is simple and can be used for rapid detection.

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徐瑞平,季美泉,丁涛,刘芸,费晓庆.低场核磁共振技术快速鉴别注水注胶肉的化学计量学研究[J].中国食品卫生杂志,2022,34(4):724-729.

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  • 收稿日期:2022-02-18
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  • 在线发布日期: 2022-08-26
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