纱布吸附-紫外灯照射法测定食品接触纸及其制品中荧光增白剂
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(1.国家食品安全风险评估中心,北京 100022;2.福建省疾病预防控制中心,福建 福州 350001)

作者简介:

屈鹏峰 男 实习研究员 研究方向为食品安全E-mail:qupengfeng@cfsa.net.cn通信作者:┣┣(中)通信作者┫┫蒋定国 男 研究员 研究方向为食品化学检测与监测E-mail:jiangdingguo@cfsa.net.cn

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基金项目:

国家自然科学基金面上项目(81072306)


Determination of fluorescent whitening agents in food contact paper by UV irradiation method combined with gauze absorption
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(China National Center for Food Safety Risk Assessment,Beijing 100022,China)

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    摘要:

    建立食品接触纸中荧光增白剂国家标准检测方法。方法 当样品有不太明显的蓝色或紫色荧光时,样品中的荧光增白剂用碱性提取溶剂提取,调节提取液为酸性,纱布吸附,在波长365 nm紫外灯照射下测定纱布的荧光强度。结果 紫外灯照射法能定性判定样品中高含量的荧光增白剂。纱布吸附结合紫外灯照射法能定性判定样品中低含量的荧光增白剂,排除样品荧光本底或者其他荧光污染物的干扰,荧光增白剂的检出限为10 mg/kg。结论 该法适合定性测定食品接触纸中荧光增白剂,操作简单,结果可靠。

    Abstract:

    To develop a national standard method for rapid determination of fluorescent whitening agents (FWAs) in food contact papers.Methods When the sample didn't obvious blue or purple fluorescence, FWAs in the sample were extracted by an alkaline solution, the extract was adjusted to acidic and absorbed by gauze,and the fluorescent intensity of the gauze was tested by UV light with the wavelength at 365 nm. Results UV irradiation method could qualitatively determination the high level of FWAs in the sample. UV irradiation method combined with gauze absorption could qualitatively determination the low level of FWAs in the sample and exclude the interference from the natural fluorescent background and other fluorescent pollutants, the limit of detection of FWAs was 10 mg/kg.Conclusion This method was simple, reliable, and suitable for the qualitative determination of FWAs in food contact papers.

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屈鹏峰,傅武胜,刘文菁,张昌胜,蒋定国.纱布吸附-紫外灯照射法测定食品接触纸及其制品中荧光增白剂[J].中国食品卫生杂志,2016,28(3):353-355.

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  • 收稿日期:2016-04-18
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  • 在线发布日期: 2016-06-02
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