To establish multiple simultaneous determination of pesticides in vegetables by GC-MS method. Method Utilizes solid-phase extraction (SPE) technology for sample pre-treatment, using GC-MS techniques for vegetables methamidophos, carbofuran, omethoate, chlorpyrifos, triazophos, cyhalothrin, cyfluthrin, cypermethrin detection, standard curve method to quantification. Results Recoveries of eight kinds of organophosphate and pyrethroid pesticides was 75.3%-110.2%, the relative standard deviation was 1.5%-5.1%, the minimum detection limit (LODS) at 1.5%-5.1%.Conclusion The method is simple and fast ,also it can meet the requirements of GC-MS’s sample solution , the recovery of the method is better and it apply to analysis the eight kinds of organophosphate and pyrethroid pesticides in vegetables.