烟台市市售散装酱腌菜中7种防腐剂含量状况调查
DOI:
作者:
作者单位:

作者简介:

董桂贤 女 副主任技师 研究方向为食品安全分析 E-mail:dgxian_77@163.com

通讯作者:

中图分类号:

基金项目:

2011年烟台市科学技术发展计划(第二批)(2011252)


Investigation of 7food preservative residuals from 300pickled vegetables in bulk at retail
Author:
Affiliation:

Fund Project:

  • 摘要
  • |
  • 图/表
  • |
  • 访问统计
  • |
  • 参考文献
  • |
  • 相似文献
  • |
  • 引证文献
  • |
  • 资源附件
  • |
  • 文章评论
    摘要:

    掌握烟台市市售散装酱腌菜中防腐剂含量情况。方法采用超高效液相色谱(UPLC)-二极管阵列检测器(PDA)法检测300份市售散装酱腌菜中7种防腐剂(山梨酸、苯甲酸、脱氢乙酸、尼泊金甲酯、尼泊金乙酯、尼泊金丙酯、尼泊金丁酯)含量。结果苯甲酸检出率为99.7%(299/300),合格率仅为37.3%(112/300),含量平均值为1.55g/kg,最大检出值5.31g/kg,是GB 2760—2011规定最大使用量的5.3倍。9种酱腌菜中,什锦菜苯甲酸平均值最高(2.34g/kg),合格率最低(13.9%)。山梨酸的检出率为68.7%(206/300),平均值0.10g/kg,最大检出值2.35g/kg,是GB 2760—2011规定最大使用量的2.3倍。脱氢乙酸检出率为25.0%(75/300),脱氢乙酸含量平均值为0.032g/kg,合格率100%。结论酱腌菜中苯甲酸含量的合格率最低,超标严重,建议应作为今后重点监督、监测的对象;加强散装酱腌菜的监管力度。

    Abstract:

    To investigate 7food preservative residuals of pickled vegetables in bulk at retail market of Yantai, and provide scientific basis for customer making decisions for such product. MethodsThe residue content of 7food preservatives including sorbic acid, benzoic acid, dehydroacetic acid were detected by ultra performance liquid chromatography with photodiode array detector (UPLC-PDA). The quality of pickled vegetable was judged by GB 2760-2011. ResultsThe detection rate of benzoic acid was 99.7% (299/300), higher than that of sorbic acid which was 68.7% (206/300), while the detection rate of dehydroacetic acid was only 25.0%. There were 188samples exceeded the benzoic acid limit of GB 2760-2011, the maximum value was 5.31g/kg which was 4.3times higher than the limit. In addition, the maximum value of sorbic acid was 2.35g/kg, 2.3times higher than the limit. Olio had the highest residual level among 300samples. The parabens were not detected in this investigation. Conclusion The content of benzoic acid was the highest and the violation rate was also the highest. We should strengthen the supervision and monitoring to control food preservative used in pickled vegetables.

    参考文献
    相似文献
    引证文献
引用本文

董桂贤,王朝霞,宫春波,张桂芳,王颖,周晓歌,杨翠云.烟台市市售散装酱腌菜中7种防腐剂含量状况调查[J].中国食品卫生杂志,2013,25(3):264-267.

复制
分享
文章指标
  • 点击次数:
  • 下载次数:
  • HTML阅读次数:
  • 引用次数:
历史
  • 收稿日期:2013-02-05
  • 最后修改日期:
  • 录用日期:
  • 在线发布日期: 2013-06-19
  • 出版日期:
《中国食品卫生杂志》邮寄地址与联系方式变更通知
关闭