Determination of epichlorohydrin residues in water from teabag by liquid-phase microextraction-gas chromatography-mass spectrometry method
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O657.7;TS272.7

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    Abstract:

    Objective To develop a method for the determination of epichlorohydrin(ECH) residues in water from teabag by liquid-phase microextraction-gas chromatography-mass spectrometry(LPME-GC-MS).Methods Epichlorohydrin in teabag water was enriched by hollow fiber liquid-phase microextraction method,separated by gas chromatography and determined qualitatively and quantitatively by mass spectrometry.Results The limit of determination was 0.18 μg/ml and the linear ranges were 0.36~7.30μg/ml(r2=0.999).Takin...

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Liu Ping, Li Liping, Li Bing, Zhao Yao, Luo Rencai, Xue Ying, Wu Guohua. Determination of epichlorohydrin residues in water from teabag by liquid-phase microextraction-gas chromatography-mass spectrometry method[J].中国食品卫生杂志,2011,23(6):506-510.

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  • Received:August 23,2011
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